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70 mL of 10 % HCl was added to the resulting concentrated solution which was then heated and stirred at a temperature of 80 to 90 0 C for 2 hours, concentrated by distillation under reduced pressure, and recrystallized from small amounts of anhydrous ethanol and acetone to afford L-carnitine hydrochloride

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That 20-minute gap at 22C is enough to compromise 1530% of peptide integrity before the first dose is ever drawn